- ▶
- Heaters/Source
- ▶
- Agilent Heaters and SensorsMass Spectrometry, Scientific Supplies & ManufacturingScientific Instrument Services 5973 Source Heater Tamper Resistant Allen Wrench 5973/5975 Quad Sensor 5985 Source Heater Assembly Agilent Interface Heater Assembly 5971 Interface Heater
- ▶
- Reference Material on InstrumentationArticle - A High Temperature Direct Probe for a Mass Spectrometer Design of a Direct Exposure Probe and Controller for use ona Hewlett-Packard 5989 Mass Spectrometer SIS AP1000 AutoProbe™ SIS AP2000 AutoProbe™ - Description of System HPP7: Direct Probe Electronics Console HPP7: Direct Probe for the Agilent (HP) 5973/5975 MSD HPP7: HP Direct Probe Application Notes HPP7: Installation Directions for the Direct Probe HPP7: Side Cover for the HP 5973 MSD HPP7: Support HPP7: Probe Inlet System for the Agilent (HP) 5973 and 5975 MSD with Automatic Indexed Stops HPP7: Theory of Operation of the Direct Probe and Probe Inlet System Direct Thermal Extraction Thermal Desorption Application Notes Environmental Thermal Desorption Application Notes Food Science Thermal Desorption Application Notes Forensic Thermal Desorption Application Notes GC Cryo-Trap Application Notes Headspace Application Notes Purge & Trap Thermal Desorption Application Notes Theory of Operation of the AutoDesorb® System AutoDesorb Notes for SIS Dealers Adsorbent Resin Application Notes Installation of the Short Path Thermal Desorption System on Agilent (HP) and Other GCs Installation of the Short Path Thermal Desorption System on a Varian 3400 GC AutoDesorb® System Development Team Thermal Desorption Applications and Reference Materials Installation of the Short Path Thermal Desorption System - TD5 Part I - Design & Operation of the Short Path ThermalDesorption System Installation Instructions for the Model 951 GC Cryo-Trap on the HP 5890 Series GC Installation Instructions for the Model 961 GC Cryo-Trap on the HP 5890 Series GC Operation of the Model 951/961 GC Cryo-Trap SIS GC Cryo Traps - Theory of Operation NIST/EPA/NIH Mass Spectral Enhancements - 1998 version (NIST98) SIMION 3D Ion Optics Class Mass Spectrometer Source Cleaning Methods MS Tip: Mass Spectrometer Source Cleaning Procedures Mass Spec Source Cleaning Procedures Micro-Mesh® Abrasive Sheets Research Papers Using New Era Syringe Pump Systems EI Positive Ion Spectra for Perfluorokerosene (PFK) Cap Liner Information How do I convert between fluid oz and milliliters? Which bottle material should I choose? Which bottle mouth should I choose? The Bottle Selection Guide CGA Connections for Gas Tanks Chemical Reaction Interface Mass Spectrometry (CRIMS)
- Lab/CleanMicro-Mesh® (Fine Cushioned Abrasive) Aluminum Oxide Cleaning Abrasive Fiberglass Cleaning Brushes Swabs and Applicators Nylon and Latex Gloves Cleaning Wipes SIS MS Source Cleaning Kits Dust-Off® Hurricane Canless Air System Wheaton Bottles Wheaton Vials Wheaton Closures Sterile Vials - Bottle, Stopper, and Cap - All Together Certified Sterile Kimble Chase Clear Serum Vials Soil Sampling Kits Crimpers and Decappers Temperature Measurement & Recording Devices Bullet Blender® Homogenizer The SW 110 Multi-Purpose Spot Welder New Era Syringe Pump Systems Ohaus MB Series Moisture Analyzers Celestron® Handheld Digital Microscope (HDM) Checkit® Pipette Accuracy Test Greenwood Lab Supplies Next Advance Lab Products Catalog Page G1
- LiteratureApplication Notes Adsorbent Resins Guide Mass Spec Tips SDS Sheets FAQ MS Calibration Compound Spectra Manuals MS Links/Labs/ Organizations MS Online Tools Flyers on Products/Services Scientific Supplies Catalog About Us NextAdvance Bullet Blender® Homogenizer Protocols Micro-Mesh® Literature Instrumentation Literature Agilent GC/MS Literature SIS News / E-Mail Newsletter NIST MS Database - Update Notifications
- ▶
- Micro-Mesh® Abrasive Sheets (This Page)
by John J. Manura
Reprinted from the "Mass Spec Source"
Scientific Instrument Services, Inc.
We have had many requests over the years for a fine grit sandpaper to clean quadrupole rods and other source parts. Most commercially available sandpapers or emery papers were too coarse or degraded too rapidly. We had several reports of some mass spec servicemen using a fine abrasive product to clean quadrupole rods, so we set out to find a source of a fine abrasive cloth for various uses in cleaning mass spectrometer parts, in particular for cleaning quadrupole rods, source slits and other source parts.
Micromesh Abrasive Sheets and File Boards
The product we eventually decided to market is known as Micro Mesh Cushioned Abrasives. This product is not like conventional abrasive sheets or sandpaper. In the case of Micro Mesh products, there is a cloth backing upon which a thin latex film is applied. The various sizes of aluminum oxide crystals are adhered onto the film in such a manner that the crystals are held in a resilient matrix, as opposed to a hard matrix. This construction allows the crystals to remain adhered to the backing even when used under pressure. What is unique about the cushioned abrasives is that they do not produce any random deep scratches. Instead, they produce an extremely uniform scratch pattern over the entire work surface. The cushioned Micro Mesh abrasives also have an extremely long life since the crystals will continue to cut effectively until they eventually become dull and lose their sharp cutting edges.
This product line was initially developed to remove scratches and to polish the acrylic windows on aircraft, but additional applications have included polishing all metals, plastics, PTFE, Vespel® and many other natural and synthetic materials.
Using Micromesh to polish out a Mass Spec Probe Rod
The normal procedure involves the use of a range of abrasive sheets. By beginning with the coarser grits and successively using finer grits, mirror finishes can be obtained. The starting grit size is determined by how deep the scratches or imperfections are in the item you are cleaning. On cleaning items such as mass spectrometer direct probes, it may be necessary to begin with the coarsest grits of abrasive to remove the deep scratches. Once you begin cleaning with a specific mesh size, you must continue the cleaning process with the next finest mesh size. It is important that none of the intermediate mesh sizes are skipped. Each successive grit size must be used in mesh size order to remove the scratches from the previous mesh size. By using the successive mesh sizes all the way down to the 12,000 mesh size, a mirror finish can be obtained. This finish is finer than the finish which could be obtained even with buffing wheels and without the mess.
The Micro-Mesh abrasives can be used either wet or dry, depending on your preference. Most users prefer to use the sheets dry without any water or other lubricant. Individual sheets can be washed out and used again. The Micro-Mesh products may cost more than ordinary sandpaper, but it produces finishes ten times finer and lasts 10 to 20 times longer. Every sheet is color coded (see Table 1) for easy reference and has the grit size written on the reverse side. Grit sizes range from 1500 grit to 12,000 grit. The higher the grit number, the finer the cutting action. The finer meshes are ideal for cleaning and polishing source slits and quadrupole rods.
Table 1 - Micromesh Abrasive Sheets and Grits Available
Product No. Description Color MM-1500 4"x 6" sheet, 1500 Grit Violet MM-1800 4"x 6" sheet, 1800 Grit Pink MM-2400 4"x 6" sheet, 2400 Grit Grey MM-3200 4"x 6" sheet, 3200 Grit Blue MM-3600 4"x 6" sheet, 3600 Grit Green MM-4000 4"x 6" sheet, 4000 Grit Yellow MM-6000 4"x 6Ó sheet, 6000 Grit Orange MM-8000 4"x 6" sheet, 8000 Grit Red MM-12000 4"x 6Ó sheet, 12000 Grit Grey
Using Micromesh File Board to Polish Source Slit
Other uses of the Micro-Mesh abrasives include the cleaning of source slits which cannot be cleaned by other materials since they would round the slit edges or remove too much metal. Cleaning quadrupole rods and other source parts is easily accomplished with minimal surface metal removal. SEM sources can also be cleaned in a similar manner.
A related product is the Micro-Mesh polishing board. This emory board sized polisher contains three of the finer grits and is ideal for reaching into tight spots, and for general instrument part cleaning where an abrasive sheet with a stiff backing is preferable. The Micro-Mesh boards are used just like the Micro-Mesh sheets, starting with the coarsest area and working toward the finest area. In our shop we use these boards for cleaning the electrodes on our spotwelders and also for cleaning filament posts. These boards are also useful for cleaning quadrupole rods. The Micro- Mesh polishing board has three different polishing surfaces on its two sides. On the side with the two sections, the dark granular gray, section is the coarsest grit and should always be used first until as many as possible of the visible scratches have been removed. The neighboring white section is the next finest grit and should be used next. This section will further smooth the rough edges and scratches caused by the first grit. Finish polishing with the opposite side of the polishing board. This side is medium gray and is the finest abrasive. This should remove the finest scratches. If not, it may be necessary to back-track to the coarser grits and repeat the operations. Remember that the polishing board is primarily for tight areas and corners and cannot be expected to do as complete a job as the Micro-Mesh sheets. It can however, do a fine job in places that are hard to reach.
Directions for using Micro-Mesh Abrasives
1 . Wipe off the object to be cleaned with a rag or cloth. Any loose, hard material left on the subject could possibly cause deep scratches which may prove difficult to remove.
2. Begin with the lowest number grit required to remove the scratches. (begin with the 1500 grit if the surface is fairly rough). Polish in straight lines completely covering the area to be polished. Further polishing with subsequent grit sizes should be done at right angles to the previous grit until the scratches and imperfections are no longer clearly visible. If the scratches or imperfections are very deep, it will probably be necessary to first sand the area with conventional 200 grit emery paper to prepare the surface for subsequent cleaning with the Micro-Mesh Abrasives.
3. After two to three minutes of polishing with the Micro-Mesh cloth, begin using the next highest grit number (next finest grit) of Micro-Mesh abrasive cloth and repeat the procedure in step 2. Remember to always work at right angles to the direction of polishing with the previous abrasive grit size.
4. Continue working with successively finer grits until the finish you desire is attained. Continuing all the way to the 12,000 grit sheet will produce a bright mirror finish on most smooth metals. A bright, shining surface can sometimes be achieved quicker depending on the metal and the initial condition of the surface.
For additional information on the availability of the Micro-Mesh products, please refer to Scientific Instrument Services complete catalog.
Also see article of source cleaning for the use of Micromesh at SIS.
Micromesh is available from SIS. See Product section for more information.