SISWEB® Application Notes

Over 80 articles on Thermal Desorption, MS Direct Probe, and SIMION, including papers we presented at PittCon, ASMS, and EAS.

Table of Contents

• Technical Bulletins
• Thermal Desorption & Cryo-Trap Notes
  • Thermal Desorption - Direct Thermal Extraction
  • Thermal Desorption - Environmental
  • Thermal Desorption - Headspace
  • Thermal Desorption - Purge and Trap
  • Thermal Desorption - Pharmaceuticals
  • Thermal Desorption - Forensics
  • Thermal Desorption - Food Science
  • Thermal Desorption - Absorbent Resins
• GC Cryo-Trap Application Notes
• MS Direct Probe Application Notes
• General Mass Spec and GC Application Notes
• SIMION (Ion Optics Software) Application Notes
• Chemical Reaction Interface Mass Spectrometry (CRIMS)

• C. Improving Sensitivity in the H.P. 5971 Mass Spectrometer - Part 1
• E. Replacing an Electron Multiplier in the Agilent (HP) 5973 MSD
• B. Elimination of "Memory Peaks" from Thermal Desorption. (781203)
• D. Improving Sensitivity in the H.P. 5971 Mass Spectrometer - Part 2
• A. Design & Operation of the Short Path Thermal Desorption System. (781201)

• A. Design & Operation of the Short Path Thermal Desorption System. (781201)
• Absorbent Resins Breakthrough Volume Data
• 1. Determination of Off-Odors and Other Volatile Organics in Food Packaging Films by Direct Thermal Analysis-GC-MS. (781301)
• 2. Detection of Arson Accelerants Using Dynamic Headspace with Tenax(R) Cartridges Thermal Desorption and Cryofocusing (781302)
• 3. Indoor Air Pollution (781303)
• 4. Direct Analysis of Spices and Coffee (781304)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 6. Direct Thermal Analysis of Plastic Food Wraps Using the Short Path Thermal Desorption System. (781306)
• 7. Chemical Residue Analysis of Pharmaceuticals Using The Short Path Thermal Desorption System. (781307)
• 8. Detection of Volatile Organic Compounds in Liquids Using the Short Path Thermal Desorption System. (781308)
• 9. Methodologies for the Quantification of Purge and Trap Thermal Desorption and Direct Thermal Analyses. (781309)
• 10. Quantification of Naphthalene in a Contaninated Pharmaceutical Product by Short Path Thermal Desorption (781310)
• 11. Flavor/Fragrance Profiles of Instant and Ground Coffees by Short Path Thermal Desorption. (PittCon 92)
• 12. Identification of the Volatile and Semi-Volatile Organics in Chewing Gums by Direct Thermal Desorption. (EAS 92)
• 13. Detection and Quantification of PNA's and PCB's in Soil by Direct Thermal Desorption (781313)
• 14. Analysis of Carbonated Beverages by P&T Thermal Desorption Quantification of Limonene and Cymene (781314)
• 16. Analysis of Indoor Air and Sources of Indoor Air Contamination by Thermal Desorption. (781316)
• 17. Identification of Volatile Organics in Wine over Time (781317)
• 18. Determination of Volatile Organic Compounds in Mushrooms (781318)
• 19. Design and Application of the SIS GC Cryo-Trap (PittCon 94)
• 20. Using Direct Thermal Desorption to Assess the Potential Pool of Styrene and 4-Phenylcyclohexane in Latex-Backed Carpets. (PittCon 94)
• 21. Detection and Identification of Volatile and Semi-Volatile Organics in Synthetic Polymers Used in Food and Pharmaceutical Packaging. (ASMS 94)
• 22. Comparison of Volatile Compounds in Latex Paints (ASMS 94)
• 23. Fragrance Qualities in Colognes (ASMS 94)
• 24. Selection of GC Guard Columns for Use with the GC Cryo-Trap (EAS 94)
• 25. Flavor and Aroma in Natural Bee Honey (EAS 94)
• 26. Volatile Organics Present in Recycled Air Aboard a Commercial Airliner (EAS 94)
• 27. Analysis of Volatile Organics in Soils by Automated Headspace GC (PittCon 95)
• 28. Analysis of Volatile Organics in Latex Paints by Automated Headspace Sampling and GC-Cryo-Focusing (PittCon 95)
• 29. Analysis of Volatile Organics in Oil Base Paints by Automated Headspace Sampling and GC Cryo-Focusing (PittCon 95)
• 30. Comparison of Cooking Oils by "Direct Thermal Extraction" and Purge and Trap GC/MS (PittCon 95)
• 31. Volatile Organic Composition in Several Cultivars of Peach (PittCon 95)
• 32. Selection and Use of Adsorbent Resins for Purge and Trap Thermal Desorption Applications (PittCon 95)
• 33. Changes in Volatiles in Milk Over Time (781333)
• 34. Selection of Thermal Desorption and Cryo-Trap Parameters in the Analysis of Teas (EAS 95)
• 35. Volatile Organic Composition of Cranberries (EAS 95)
• 36. Identification of Volatile Organic Compounds in a New Automobile (EAS 95)
• 37. Volatile Organic Emissions from Automobile Tires (EAS 95)
• 38. A New Micro Cryo-Trap for Trapping of Volatiles at the front of a GC Capillary Column (PittCon 96)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics
• 40. Composition of Septa by Direct Thermal Extraction
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 42. The Influence of Pump Oil Purity on Roughing Pumps
• 43. Volatile Organic Composition in Blueberry
• 54. Identification of Volatile Organic Compounds in Office Products
• 55. Seasonal Variation in Flower Volatiles
• 56. Mass Spec Maintenance & Cleaning Utilizing Micro Mesh Abrasive Sheets
• 57. Aroma Profiles of Various Lavandula Species (PittCon 97)
• 60. Programmable Temperature Ramping of Samples Analyzed via Direct Thermal Extraction GC/MS (EAS 97)
• 63. Organics in Printer Toners using Thermal Desorption
• 64. Comparison of Various GC/MS Techniques for the Analysis of Black Pepper (PittCon 98)
• 65. Determination of Ethylene by Adsorbent Trapping and Thermal Desorption GC (PittCon 98)
• 71. Flavor Profile Determination of Rice Samples Using Thermal Desorption (ASMS 98)
• 73. The Analysis of Perfumes and Their Effect on Indoor Air Polution (EAS 98)
• 75. An Apparatus for Sampling Volatile Organics from Live Plant Material Using Short Path Thermal Desorption (EAS 98)
• 77. The Determination of Volatile Organics in Vacuum System Components (ASMS 97)
• 79. Volatile Organic Compounds From Electron Beam Cured and Partially Electron Beam Cured Packaging Using Automated Short Path Thermal Desorption (PittCon 99)
• 80. Design, Development and Testing of a Microprocessor Controlled Automated Short Path Thermal Desorption Apparatus (PittCon 99)
• 82. Vacuum Pump Exhaust Filters, Part I, A Two Stage Vacuum Pump EExhaust Filter System (ASMS 2000)
• 83. Vacuum Pump Exhaust Filters, Part II, Oil Mist Eliminators
• 84. Vacuum Pump Exhaust Filters, Part III, charcoal Exhaust Traps
• 88. Analysis of Silicone Contaminants on Electronic Components by Thermal Desorption GC-MS (ASMS 99)
• 93. Detection of Benzene in Carbonated Beverages with Purge & Trap Thermal Desorption GC/MS (Pittcon2007)
• 94. Detection of Nepetalactone in the Nepeta Cataria Plant by Thermal Desorption GC/MS (ASMS2007)
• 95. Detection of Explosives on Clothing Material by Direct and Air Sampling Thermal Desorption GC/MS (ASMS2007)

• 1. Determination of Off-Odors and Other Volatile Organics in Food Packaging Films by Direct Thermal Analysis-GC-MS. (781301)
• 4. Direct Analysis of Spices and Coffee (781304)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 6. Direct Thermal Analysis of Plastic Food Wraps Using the Short Path Thermal Desorption System. (781306)
• 7. Chemical Residue Analysis of Pharmaceuticals Using The Short Path Thermal Desorption System. (781307)
• 9. Methodologies for the Quantification of Purge and Trap Thermal Desorption and Direct Thermal Analyses. (781309)
• 10. Quantification of Naphthalene in a Contaninated Pharmaceutical Product by Short Path Thermal Desorption (781310)
• 11. Flavor/Fragrance Profiles of Instant and Ground Coffees by Short Path Thermal Desorption. (PittCon 92)
• 12. Identification of the Volatile and Semi-Volatile Organics in Chewing Gums by Direct Thermal Desorption. (EAS 92)
• 13. Detection and Quantification of PNA's and PCB's in Soil by Direct Thermal Desorption (781313)
• 20. Using Direct Thermal Desorption to Assess the Potential Pool of Styrene and 4-Phenylcyclohexane in Latex-Backed Carpets. (PittCon 94)
• 21. Detection and Identification of Volatile and Semi-Volatile Organics in Synthetic Polymers Used in Food and Pharmaceutical Packaging. (ASMS 94)
• 30. Comparison of Cooking Oils by "Direct Thermal Extraction" and Purge and Trap GC/MS (PittCon 95)
• 37. Volatile Organic Emissions from Automobile Tires (EAS 95)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics
• 40. Composition of Septa by Direct Thermal Extraction
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 94. Detection of Nepetalactone in the Nepeta Cataria Plant by Thermal Desorption GC/MS (ASMS2007)
• 95. Detection of Explosives on Clothing Material by Direct and Air Sampling Thermal Desorption GC/MS (ASMS2007)

• 2. Detection of Arson Accelerants Using Dynamic Headspace with Tenax(R) Cartridges Thermal Desorption and Cryofocusing (781302)
• 3. Indoor Air Pollution (781303)
• 8. Detection of Volatile Organic Compounds in Liquids Using the Short Path Thermal Desorption System. (781308)
• 13. Detection and Quantification of PNA's and PCB's in Soil by Direct Thermal Desorption (781313)
• 16. Analysis of Indoor Air and Sources of Indoor Air Contamination by Thermal Desorption. (781316)
• 26. Volatile Organics Present in Recycled Air Aboard a Commercial Airliner (EAS 94)
• 27. Analysis of Volatile Organics in Soils by Automated Headspace GC (PittCon 95)
• 36. Identification of Volatile Organic Compounds in a New Automobile (EAS 95)
• 37. Volatile Organic Emissions from Automobile Tires (EAS 95)
• 38. A New Micro Cryo-Trap for Trapping of Volatiles at the front of a GC Capillary Column (PittCon 96)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics
• 40. Composition of Septa by Direct Thermal Extraction
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 42. The Influence of Pump Oil Purity on Roughing Pumps

• 27. Analysis of Volatile Organics in Soils by Automated Headspace GC (PittCon 95)
• 28. Analysis of Volatile Organics in Latex Paints by Automated Headspace Sampling and GC-Cryo-Focusing (PittCon 95)
• 29. Analysis of Volatile Organics in Oil Base Paints by Automated Headspace Sampling and GC Cryo-Focusing (PittCon 95)
• 38. A New Micro Cryo-Trap for Trapping of Volatiles at the front of a GC Capillary Column (PittCon 96)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics

• 2. Detection of Arson Accelerants Using Dynamic Headspace with Tenax(R) Cartridges Thermal Desorption and Cryofocusing (781302)
• 3. Indoor Air Pollution (781303)
• 8. Detection of Volatile Organic Compounds in Liquids Using the Short Path Thermal Desorption System. (781308)
• 14. Analysis of Carbonated Beverages by P&T Thermal Desorption Quantification of Limonene and Cymene (781314)
• 16. Analysis of Indoor Air and Sources of Indoor Air Contamination by Thermal Desorption. (781316)
• 17. Identification of Volatile Organics in Wine over Time (781317)
• 18. Determination of Volatile Organic Compounds in Mushrooms (781318)
• 20. Using Direct Thermal Desorption to Assess the Potential Pool of Styrene and 4-Phenylcyclohexane in Latex-Backed Carpets. (PittCon 94)
• 21. Detection and Identification of Volatile and Semi-Volatile Organics in Synthetic Polymers Used in Food and Pharmaceutical Packaging. (ASMS 94)
• 22. Comparison of Volatile Compounds in Latex Paints (ASMS 94)
• 23. Fragrance Qualities in Colognes (ASMS 94)
• 25. Flavor and Aroma in Natural Bee Honey (EAS 94)
• 26. Volatile Organics Present in Recycled Air Aboard a Commercial Airliner (EAS 94)
• 30. Comparison of Cooking Oils by "Direct Thermal Extraction" and Purge and Trap GC/MS (PittCon 95)
• 31. Volatile Organic Composition in Several Cultivars of Peach (PittCon 95)
• 32. Selection and Use of Adsorbent Resins for Purge and Trap Thermal Desorption Applications (PittCon 95)
• 33. Changes in Volatiles in Milk Over Time (781333)
• 34. Selection of Thermal Desorption and Cryo-Trap Parameters in the Analysis of Teas (EAS 95)
• 35. Volatile Organic Composition of Cranberries (EAS 95)
• 38. A New Micro Cryo-Trap for Trapping of Volatiles at the front of a GC Capillary Column (PittCon 96)
• 42. The Influence of Pump Oil Purity on Roughing Pumps
• 43. Volatile Organic Composition in Blueberry
• 93. Detection of Benzene in Carbonated Beverages with Purge & Trap Thermal Desorption GC/MS (Pittcon2007)

• 1. Determination of Off-Odors and Other Volatile Organics in Food Packaging Films by Direct Thermal Analysis-GC-MS. (781301)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 7. Chemical Residue Analysis of Pharmaceuticals Using The Short Path Thermal Desorption System. (781307)
• 9. Methodologies for the Quantification of Purge and Trap Thermal Desorption and Direct Thermal Analyses. (781309)
• 10. Quantification of Naphthalene in a Contaninated Pharmaceutical Product by Short Path Thermal Desorption (781310)

• 1. Determination of Off-Odors and Other Volatile Organics in Food Packaging Films by Direct Thermal Analysis-GC-MS. (781301)
• 2. Detection of Arson Accelerants Using Dynamic Headspace with Tenax(R) Cartridges Thermal Desorption and Cryofocusing (781302)
• 3. Indoor Air Pollution (781303)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 6. Direct Thermal Analysis of Plastic Food Wraps Using the Short Path Thermal Desorption System. (781306)
• 7. Chemical Residue Analysis of Pharmaceuticals Using The Short Path Thermal Desorption System. (781307)
• 20. Using Direct Thermal Desorption to Assess the Potential Pool of Styrene and 4-Phenylcyclohexane in Latex-Backed Carpets. (PittCon 94)
• 21. Detection and Identification of Volatile and Semi-Volatile Organics in Synthetic Polymers Used in Food and Pharmaceutical Packaging. (ASMS 94)
• 22. Comparison of Volatile Compounds in Latex Paints (ASMS 94)
• 23. Fragrance Qualities in Colognes (ASMS 94)
• 27. Analysis of Volatile Organics in Soils by Automated Headspace GC (PittCon 95)
• 28. Analysis of Volatile Organics in Latex Paints by Automated Headspace Sampling and GC-Cryo-Focusing (PittCon 95)
• 29. Analysis of Volatile Organics in Oil Base Paints by Automated Headspace Sampling and GC Cryo-Focusing (PittCon 95)
• 37. Volatile Organic Emissions from Automobile Tires (EAS 95)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics
• 40. Composition of Septa by Direct Thermal Extraction
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 42. The Influence of Pump Oil Purity on Roughing Pumps
• 95. Detection of Explosives on Clothing Material by Direct and Air Sampling Thermal Desorption GC/MS (ASMS2007)

• 1. Determination of Off-Odors and Other Volatile Organics in Food Packaging Films by Direct Thermal Analysis-GC-MS. (781301)
• 4. Direct Analysis of Spices and Coffee (781304)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 6. Direct Thermal Analysis of Plastic Food Wraps Using the Short Path Thermal Desorption System. (781306)
• 8. Detection of Volatile Organic Compounds in Liquids Using the Short Path Thermal Desorption System. (781308)
• 9. Methodologies for the Quantification of Purge and Trap Thermal Desorption and Direct Thermal Analyses. (781309)
• 11. Flavor/Fragrance Profiles of Instant and Ground Coffees by Short Path Thermal Desorption. (PittCon 92)
• 12. Identification of the Volatile and Semi-Volatile Organics in Chewing Gums by Direct Thermal Desorption. (EAS 92)
• 14. Analysis of Carbonated Beverages by P&T Thermal Desorption Quantification of Limonene and Cymene (781314)
• 17. Identification of Volatile Organics in Wine over Time (781317)
• 18. Determination of Volatile Organic Compounds in Mushrooms (781318)
• 21. Detection and Identification of Volatile and Semi-Volatile Organics in Synthetic Polymers Used in Food and Pharmaceutical Packaging. (ASMS 94)
• 25. Flavor and Aroma in Natural Bee Honey (EAS 94)
• 30. Comparison of Cooking Oils by "Direct Thermal Extraction" and Purge and Trap GC/MS (PittCon 95)
• 31. Volatile Organic Composition in Several Cultivars of Peach (PittCon 95)
• 33. Changes in Volatiles in Milk Over Time (781333)
• 35. Volatile Organic Composition of Cranberries (EAS 95)
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 43. Volatile Organic Composition in Blueberry
• 93. Detection of Benzene in Carbonated Beverages with Purge & Trap Thermal Desorption GC/MS (Pittcon2007)

• Absorbent Resins Breakthrough Volume Data
• 32. Selection and Use of Adsorbent Resins for Purge and Trap Thermal Desorption Applications (PittCon 95)
• 34. Selection of Thermal Desorption and Cryo-Trap Parameters in the Analysis of Teas (EAS 95)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics

• 19. Design and Application of the SIS GC Cryo-Trap (PittCon 94)
• 24. Selection of GC Guard Columns for Use with the GC Cryo-Trap (EAS 94)
• 27. Analysis of Volatile Organics in Soils by Automated Headspace GC (PittCon 95)
• 28. Analysis of Volatile Organics in Latex Paints by Automated Headspace Sampling and GC-Cryo-Focusing (PittCon 95)
• 29. Analysis of Volatile Organics in Oil Base Paints by Automated Headspace Sampling and GC Cryo-Focusing (PittCon 95)
• 30. Comparison of Cooking Oils by "Direct Thermal Extraction" and Purge and Trap GC/MS (PittCon 95)
• 31. Volatile Organic Composition in Several Cultivars of Peach (PittCon 95)
• 34. Selection of Thermal Desorption and Cryo-Trap Parameters in the Analysis of Teas (EAS 95)
• 36. Identification of Volatile Organic Compounds in a New Automobile (EAS 95)
• 37. Volatile Organic Emissions from Automobile Tires (EAS 95)
• 38. A New Micro Cryo-Trap for Trapping of Volatiles at the front of a GC Capillary Column (PittCon 96)
• 39. Comparison of Sensitivity of Headspace GC, Purge and Trap Thermal Desorption and Direct Thermal Extraction Techniques for Volatile Organics
• 40. Composition of Septa by Direct Thermal Extraction
• 41. Hydrocarbon Production in Pine by Direct Thermal Extraction
• 42. The Influence of Pump Oil Purity on Roughing Pumps
• 43. Volatile Organic Composition in Blueberry

• 44. The Design of a New Direct Probe Inlet for a Mass Spectrometer
• 48. Demonstration of Sensitivity Levels of Caffeine for a New Direct Probe and Inlet for the HP 5973 MSD
• 49. Analysis of Cocaine Utilizing a New Direct Insertion Probe on a Hewlett Packard 5973 MSD
• 50. The Analysis of Multiple Component Drug Samples Using a Direct Probe Interfaced to the HP 5973 MSD
• 58. Direct Probe Analysis and Identification of Multicomponent Pharmaceutical Samples via Electron Impact MS (ASMS 97)
• 61. Analysis of Sugars via a New DEP Probe Tip for use with the Direct Probe on the HP5973 MSD (ASMS 97)
• 62. Analysis of Polymer Samples Using a Direct Insertion Probe and EI Ionization (ASMS 97)
• 66. Optimization of Probe Tip Design on a Mass Spectrometer Direct Insertion Probe (ASMS 98)
• 81. Rapid Bacterial Chemotaxonomy by Direct Probe/MSD (PittCon 99)
• 87. Design and Development of an Automated Direct Probe for a Mass Spectrometer (PittCon 2000)
• 89. Quantitation of Organics via a Mass Spectrometer Automated Direct Probe
• 90. An Automated MS Direct Probe for use in an Open Access Environment
• 91. AutoProbe DEP Probe Tip Temperatures

• C. Improving Sensitivity in the H.P. 5971 Mass Spectrometer - Part 1
• D. Improving Sensitivity in the H.P. 5971 Mass Spectrometer - Part 2
• 3. Indoor Air Pollution (781303)
• 4. Direct Analysis of Spices and Coffee (781304)
• 5. Direct Analysis Using the Short Path Thermal Desorption System: (781305)
• 72. 1998 Version of the NIST/EPA/NIH Mass Spectral Library - NIST98
• 78. A New solution to Eliminate MS mown-time with no-tool-changing analytical GC Columns (PittCon 99)
• 82. Vacuum Pump Exhaust Filters, Part I, A Two Stage Vacuum Pump EExhaust Filter System (ASMS 2000)
• 83. Vacuum Pump Exhaust Filters, Part II, Oil Mist Eliminators
• 84. Vacuum Pump Exhaust Filters, Part III, charcoal Exhaust Traps
• 85. Replacing an electron Multiplier in the Agilent (HP) 5973 MSD
• 92. Yttria Coated Mass Spectrometer Filaments

• 45. Application of SIMION 6.0 to Filament Design for Mass Spectrometer Ionization Sources (ASMS 96)
• 46. Delayed extraction and Laser Desorption: Time-lag Focusing and Beyond (ASMS 96)
• 47. The Application of SIMION 6.0 to Problems in Time-of-Flight Mass Spectrometry (ASMS 96)
• 52. Computer Modeling of Ion Optics in Time-of-Flight Mass Spectrometry Using SIMION 3D (EAS 96)
• 53. SIMION 3D v6.0 Ion Optics Simulation Software (AVS 96)
• 59. Experimental Results and SIMION 3D Modeling of the Efects of Grids in TOF Mass Spectrometry (ASMS 97)
• 69. Application of SIMION 6.0 to the Study of Finkelstein - Part I (EAS 97)
• 70. A Revisitation of the Finkelstein Ion Source using SIMION 3D - Part II
• 74. Examination of Source Design in Electrospray-TOF Using SIMION 3D
• 86. Simulation of a Unique Cylindrical Quadrupole Mass Analyzer Using SIMION 7.0.

• 51. Development and Characterization of a New Chemical Interface for the Detection of Nonradioisotopically Labeled Analytes Using Mass Spectrometry (CRIMS) (EAS 96)
• 67. Using Chemical Reaction Interface (CRIMS) to Monitor Bacteria Transport in Situ (PittCon 98)
• 68. Using a Plug In UV-Vis Spectrometer to Monitor the Plasma Conditions in a GC CRIMS (EAS 98)
• 76. Determination of the Sensitivity of a CRIMS System (ASMS 98)

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