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Pages in this section: A60 A61 A62 (all shown below)
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Direct Insertion Probe for Agilent 5973 & 5975
A60
Scientific Instrument Services, Inc.
™
Phone: 908-788-5550
www.sisweb.com/catalog/08/A60
D
irect Probe sample analysis can be accomplished on the
Agilent 5973 &5975 MSD with the new Direct Probe Inlet
System from Scientific Instrument Services
™
. The probe
inlet mounts onto the GC/MS transfer line port and uses an indexed
probe introduction guide to permit the direct insertion and removal
of the probe into the MSD source without venting the MSD or scor-
ing the probe rod. The probe can be either heated ballistically at
ramp rates in excess of 500 degrees per minute or can be temper-
ature programmed with up to 25 ramp rate levels. The probe tem-
peratures, ramp rates, hold times, start and stop are all PC con-
trolled and fully integrated with the Agilent ChemStation
™
software.
This permits the storage of the probe analysis parameters in the
sample data files and the method files.
The SIS
™
probe for the Agilent 5973 & 5975 MSD is only 1/4" in
diameter which enables it to easily slide through the probe sealing
system and into the MSD. It is light in weight and comfortably fits in
your hand for ease of use. The Probe tip with sample vial can be
heated up to 450°C either ballistically or in the programmable
mode. In the ballistic mode it will ramp up to temperature in excess
of 500 degrees per minute or alternatively it can be used in the
temperature ramp mode which has 25 levels of ramping capabilities
to provide for the ultimate control of probe tip temperature. For
cooling the probe, compressed air is used. This permits the cooling
of the probe after sample analysis and before the probe is removed
from the MSD through the vacuum seals. This prevents damage to
the probe inlet vacuum seals.
The probe tip incorporates a small spring to gently hold the
sample vial in place. The probe is designed for using glass flared
sample vials. These flared sample vials permit the efficient
introduction of samples (both solid and liquid) into the sample vials
and permit the easy insertion and removal of the sample vials from
the probe tip without breakage.
Direct Insertion Probe for the Agilent 5973 and 5973N & 5975 MSD
Direct Probe for the Agilent 5973 & 5975
System Features
•
Easy to install - mounts on the GC/MS Inlet
Port
•
PC window for the control of temperatures
and ramp rates
•
Ballistic ramp rate >500 degrees per minute
•
Up to 25 levels of programmable
temperature ramping
•
Probe PC control software fully integrated
with the Agilent ChemStation™ software
•
Can be used with either the turbo pump or
diffusion pump version of 5973 & 5975
Complete Direct Probe System mounted on the
Agilent 5973 MSD
Probe Tip with sample vial ready for introduction into
the MSD
Direct Insertion Probe and Probe Inlet System
Also See:
Also See:
WEB Site for more information
and accessories.
www.sisweb.com/ms/hp/5973prob.htm
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A61
Direct Insertion Probe for Agilent 5973 & 5975
Scientific Instrument Services, Inc.
™
FAX: 908-806-6631
www.sisweb.com/catalog/08/A61
Part No.
Description
HPP7 Part #HPP7--Click to order
Current Price: $9900.00
Unit of Measure: EA
Est. Ship Weight=50 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Probe Inlet System
S12A Part #S12A--Click to order
Current Price: $105.00
Unit of Measure: PK
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Flared Sample Vials, 100
S12C Part #S12C--Click to order
Current Price: $498.00
Unit of Measure: PK
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Flared Sample Vials, 500
S12B Part #S12B--Click to order
Current Price: $945.00
Unit of Measure: PK
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Flared Sample Vials, 1000
HPP7007 Part #HPP7007--Click to order
Current Price: $79.00
Unit of Measure: PK
Est. Ship Weight=0.25 lbs
Quantity in Stock=5
Replacement Inlet Seal Set
Probe Inlet System
The SIS
™
Probe Inlet System mounts on the GC/MS Transfer
line port on the Agilent 5973 & 5975 MSD to permit the quick and
easy introduction of the SIS 1/4" diameter direct probe through the
MSD Vacuum manifold and into the MSD source. It incorporates an
indexed dual guide rod system that accurately guides the probe
through the vacuum system valves. The guide rods are indexed at
three positions in addition to the fully inserted and fully extracted
positions.
Load - fully extended - probe load position
Stop 1 - at the first vacuum seal - to permit the rough pump-out
of the probe inlet seals
Stop 2 - at the second vacuum seal - to enable the user to open
the isolation valve
Stop 3 - 1 cm from the source - cooling position after the
sample is finished
Run - fully inserted - sample analysis Run position
After the probe locks in at one of the indexed stop positions, the
lock release lever is pulled up to enable the probe to be inserted to
the next indexed position. This accurate positioning and locking of
the probe in set positions prevents closing the isolation valve on
the probe (which would score or bend the probe rod).
The probe sealing system consists of the SIS dual PTFE seal-
ing system which will provide for excellent vacuum sealing around
the probe rod along with long seal life. If the seals need to be
replaced a seal extraction tool is included to enable the quick
removal and replacement of the seals without venting the MSD.
The 1/4" turn ball isolation valve permits the introduction of the
probe through this valve and into the MSD source.
PC Window for the Control of the SIS Direct Probe
for the Agilent 5973 & 5975 MSD
The user interface for the control and monitoring of the direct
probe for the Agilent 5973 & 5975 probe is via software on the PC.
This window is fully integrated with the Agilent ChemStation™ soft-
ware. The PC software controls the direct probe electronics con-
sole via an RS232 interface to download the values entered
through the PC window to control the actual temperature of the
probe. The probe can be operated in the ballistic mode with ramp
rates greater than 500° per minute. In the programmable mode the
user inputs the ramp rate, the final temperature and the duration
time (hold time). Temperature program rates up to 400° per minute
can be used to control the temperature of the probe between 25
and 450 °C. Up to 25 levels of programmable ramping steps are
permitted through this PC interface. A visual graphic presentation of
the temperature profile indicates the ramp and hold temperatures
as a function of time. In addition the status portion of the screen
shows the probe status, time of analysis, the target and actual
probe temperatures and the power requirements to heat the probe
(Heating Load). Controls are also present to permit the start and
cool down (stop) of the probe from the PC window. These start and
stop manual controls are also available on the front of the electron-
ics console. In addition to heating the probe, the probe is automat-
ically cooled at the end of the sample analysis using compressed
air controlled by a solenoid valve in the direct probe electronics
console. This will cool the probe to enable the removal of the probe
through the vacuum sealing system.
The probe inlet system (Part #HPP7 Part #HPP7--Click to order
Current Price: $9900.00
Unit of Measure: EA
Est. Ship Weight=50 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
) includes the direct probe,
the probe inlet, probe controller, software, vacuum pump, tools
and other accessories.
Probe
Sealing
System
Delrin
Insert
Isolation
Ball Valve
MSD
Flange
Mount
PTFE
Vacuum
Seal
Vent
Spacer
O’Ring
Seal
O’Ring
Seal
Mass Spec Probe
Knurled Nut
Pump Out Valve
Mounting
Bracket
PTFE
Vacuum
Seal
Initial
1
20
25
25
25
10%
0:00
400
300
200
100
0
0
2
4
6
8
10
12
14
100
400
100
2.00
3.00
1.00
2
Cool
Cooling
Ballistic
Status
Actual
Target
Heating
Load
Run Time
Ready
Resume
Cool
Probe Control Options Help
Start
Time (minutes)
SIS Probe Control
SIS Probe Control
T
emperature
(°C)
Rate
(°C/min)
Temp
(°C)
Duration
(minutes)
Connect
Run
Stop 3
Stop 2
Stop 1
Load
Ordering Information
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DCI/DEP & CAL Gas Probe
A62
Scientific Instrument Services, Inc.
™
Phone: 908-788-5550
www.sisweb.com/catalog/08/A62
S.I.S.
™
DCI/DEP Probe
T
he S.I.S. DCI/DEP probe is designed for use on the Agilent 5989 mass spectrometer as well as other instruments which use a
1/2" probe inlet. The DCI probe utilizes a replaceable filament wire at the end of the probe to both hold and heat the sample. In
this technique a current is supplied to the filament wire which directly heats the sample. The temperature of the sample is
controlled by limiting the value of the current supplied to the filament. The probe tip filaments simply plug in for easy replacement by the
user. The probe comes with the valve and fittings necessary for introduction of the CI reagent gas through the probe.
The S.I.S. Model PC-3 Part #PC3--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
 power supply is designed for use with the S.I.S. DCI probe. An LCD display shows all necessary parameters
and the current status of the probe. Data system remote start capability is included.
Glass vial
Calibration Gas Probe
T
hese new Calibration Gas Probes are designed for the quick and accurate introduction of liquid or gas samples directly into the
Mass Spec source via the probe inlet. The calibration gas or fluid (or any liquid sample) is placed in the removable glass vial
in the handle of the probe. The calibration vials can be quickly and easily changed to permit the analysis of multiple liquid sam-
ples. The vials hold approximately 2.0 ml of liquid. The rate of flow of the sample into the mass spec source is regulated via the microfine
metering valve on the end of the probe handle.
The Calibration Gas Probe offers the advantage for the analysis of multiple liquid samples quickly and easily. In addition, when you
are done calibrating the mass spectrometer with the calibration fluid of choice, the probe (and the source of
calibration fluid) is removed from the mass spectrometer.
CAL1 Part #CAL1--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Part No.
Description
CAL1 Part #CAL1--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Cal Gas Probe for Agilent5989
CAL2 Part #CAL2--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Cal Gas Probe for Thermoquest TSQ
CAL3 Part #CAL3--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Cal Gas Probe for Thermoquest GCQ
CV1 Part #CV1--Click to order
Current Price: $26.00
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Cal Gas Vial
Standard Direct Probe
T
he S.I.S. direct insertion probe, for use on the Agilent 5989 and other mass spectrometers which have a 1/2" probe inlet, pro-
vides the user with greater flexibility and much faster ramp rates than the standard Agilent DIP probe. This is accomplished by
positioning the heater at the tip of the probe where it is in direct contact with the sample vial. The maximum ramp rate is approx-
imately 200°C/min. when used with our separate temperature controller. The controller is equipped with a remote start switch and cable
to allow the remote starting of the mass spectrometer from the PC-1 Part #PC1--Click to order
Current Price: $1600.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
 controller. The probe design provides for much faster heating of the
sample and also faster cool down of the probe which allows for faster sample throughput. The maximum temperature of the probe is
400°C.
Scientific Instrument Services
™
has developed a new High Temperature Direct Insertion Probe (HT-DIP). The probes can be used from
ambient temperature up to 800°C with ballistic temperature ramp of over 700°C/min. Available for Agilent and Thermo Systems.
Part No.
Description
HPP2A Part #HPP2A--Click to order
Current Price: $3360.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
DCI Probe for Agilent5989
PC-3 Part #PC3--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Power Supply for DCI Probe
PC3-220 Part #PC3220--Click to order
Current Price: $2700.00
Unit of Measure: EA
Est. Ship Weight=6 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Power supply for DCI Probe, 220v
HP-DEP Part #HPDEP--Click to order
Current Price: $115.00
(6 or more: 5% off)
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Replacement DCI Filament Tip
HP-DEP1 Part #HPDEP1--Click to order
Current Price: $120.00
(6 or more: 5% off)
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Glass Encapsulated Filament Tip
HP-DEP2 Part #HPDEP2--Click to order
Current Price: $115.00
(6 or more: 5% off)
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Extra Long DEP Filament Tip
HP-DEP3 Part #HPDEP3--Click to order
Current Price: $115.00
(6 or more: 5% off)
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Ribbon Filament Tip
Microfine needle valve
Part No.
Description
HPP1 Part #HPP1--Click to order
Current Price: $4900.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
DIP Probe for Agilent 5989
PC1 Part #PC1--Click to order
Current Price: $1600.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
DIP Probe Temperature Controller
PC1-220 Part #PC1220--Click to order
Current Price: $1600.00
Unit of Measure: EA
Est. Ship Weight=6 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
DIP Probe Controller, 220v
GPT1 Part #GPT1--Click to order
Current Price: $115.00
Unit of Measure: EA
Est. Ship Weight=0.25 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
Gold Plated Insert
HPP4 Part #HPP4--Click to order
Current Price: $5300.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
High Temperature DIP for Agilent5989
PC2 Part #PC2--Click to order
Current Price: $2050.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
High Temperature DIP Controller for
Agilent5989
PC2-220 Part #PC2220--Click to order
Current Price: $2050.00
Unit of Measure: EA
Est. Ship Weight=6 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
High Temperature DIP Controller for
Agilent5989, 220v
FP15 Part #FP15--Click to order
Current Price: $5300.00
Unit of Measure: EA
Est. Ship Weight=3 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
High Temp. DIP for Finn. TSQ
PC2F Part #PC2F--Click to order
Current Price: $2050.00
Unit of Measure: EA
Est. Ship Weight=6 lbs
Not in stock. Standard lead time for out-of-stock items is approximately two weeks.
High Temp. DIP Controller for Finn. TSQ
S17A Part #S17A--Click to order
Current Price: $105.00
Unit of Measure: PK
Est. Ship Weight=0.25 lbs
Quantity in Stock=2
Flared Sample Vials, pk. 100
Related information may be found on the following pages of our web site:
PageParts
HPP7: Direct Probe Inlet System Ordering Information, pg A61HPP7007, HPP7, S12A, S12B, S12C
Probe Inlet for HP5989 MS with Automatic Stops - A67HPP1, HPP2A
Finnigan TSQ High Temperature Probe & ControllerFP15, PC2F
GCQ Probe and Probe InletPC2, S17A
Flared Pyrex Sample Vials for Finnigan and SIS MS Probe, pg. A69S17A
Hewlett Packard 5989 Probe Inlet with stopsHPP1, HPP2A
Direct Insertion Probe for HP MS with Controller - A62FP15, GPT1, HPP1, HPP4, PC1, PC1220, PC2, PC2220, PC2F, S17A
Calibration Gas Probe for HP and Finnigan MSCAL1, CAL2, CV1
High Temperature Direct Probe for HP and Finnigan MSFP15, HPP4, PC2, PC2F, S17A
DCI/DEP Probe for HP and Other MSHPDEP, HPDEP1, HPDEP2, HPDEP3, HPP2A, PC3
Page Number: [ previous page next page ]
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