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Thermal Desorption Sample Loader

For loading internal standards or liquid samples onto GLT Desorption Tubes

Sample Loader
Desorption Tube Injection Head for S.I.S. Thermal Desorption Tubes

This new Desorption Tube Injection Head works much like the injection port on a Gas Chromatograph. This device is used to inject or load liquid samples directly into the S.I.S. Thermal Desorption Tubes, forcing the syringe contents onto the adsorbent resins in the desorption tube without any loss of sample due to back evaporation. This technique can be used to quantitatively inject the standards onto the adsorbent trap without any sample loss. In addition the solvents used for injection can be purged from the adsorbent resins by continued purging with the carrier gas. Constructed of stainless steel, the entire purge head can be baked out in an oven to thoroughly clean and remove contaminants.

The Desorption Tube Injection Head consists of a septum nut with septum for the introduction of the syringe needle and sample. A purge gas (carrier gas) flushes around the syringe needle purging any sample thereon to be carried onto the desorption tube resins. The S.I.S. desorption tube screws into the Desorption Tube Injection Head and a seal is made via the standard 1/4" PTFE Seal. The purge gas fitting consists of a standard 1/16" Swagelok fitting. The Desorption Tube Injection Head Body is 0.5" in diameter and is designed to clamp into the same ring clamp used for the S.I.S. Sample Purge Head and can be mounted on the Sample Purge System ringstand or other suitable stand.

sample loader theory

Tech Tip Injecting samples and internal standards onto adsorbent resins using the Direct Injection Adaptor assures that all of the sample is delivered to the adsorbent resin bed.


Indicate # of packages.

Part No. UOMOD (in)ID (in)Thickness (in)Cap SealTop SealNeedle SealAcc Sealspkg of est
wt.
Quantity
In Stock
Price / Pkg. Quantity (pkg)
to order
783092 Direct Injection Adaptor for Liquid Sample Loading, does not include GLT tube
EA------------------------ 0.25 6$235.00
1
041844 SGE Septa, 9 mm dia. for Direct Injection Adaptor, pkg of 50
PK------------------------ 0.25 0(#)CALL
1
781004 PTFE Washers
PK0.210.120.06YesYesYesYes10 0.25 82$9.24
1
789019 PEEK (R) connector tubing for purge gas line, 1/16in O.D. per foot
Foot------------------------ 0.25 0(#)$8.50
1
783020 Clamp, ring stand type for Direct Injection Adaptor
EA------------------------ 0.25 8$49.00
1
(#) Standard lead-time for out-of-stock items is approximately two weeks.
shopping cart Ordering information. International (non-US) prices available through your local dealer.
Peek is a registered trademark of Upchurch Scientific.
SIS Catalog Cross Reference
Page #Part Numbers
C11 - AutoDesorbâ„¢ 781004
C12 - Short Pathâ„¢ Thermal Desorption Tubes 781004
C14 - TD1/TD2/TD3/TD4/TD5 Needles and Seals 781004
C27 - Purge & Trap System 783020, 789019
C28 - Purge & Trap System Purge Heads 781004
C31 - Temperature Controller & Heater Sleeves 789019
C32 - Purge and Trap System 781004
C33 - Thermal Desorption Accessories 041844, 781004, 783020, 783092, 789019
D40 - SGE GC Injection Port Septa 041844
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